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高效氟吡甲禾灵_72619-32-0
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高效氟吡甲禾灵

BW902030 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 72619-32-0 100mg {{goodObj.date}} 秦境 {{item.norm}} 97.8% {{inventory}}
高效氟吡甲禾灵介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.Uncertainty

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external7 accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

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国家标准《食品安全国家标准 植物源性食品中208种农药及其代谢物残留量的测定 气相色谱-质谱联用法》
标准名称及标准号GB 23200.113-2018
适用范围适用于植物源性食品中高效氟吡甲禾灵及其他207种农药残留的检测。
核心检测方法气相色谱-质谱联用法(GC-MS/MS),采用内标法或外标法定量。
检出限与定量限高效氟吡甲禾灵的检出限(LOD)为0.01 mg/kg,定量限(LOQ)为0.05 mg/kg。
质控样品要求空白样品添加回收率需满足70%-120%,平行样品相对标准偏差(RSD)≤15%。
关键实验步骤1. 样品提取:乙腈振荡提取;2. 净化:固相萃取(SPE)或QuEChERS法;3. 仪器分析:GC-MS/MS梯度分离与多反应监测(MRM)。
特别说明高效氟吡甲禾灵易受基质干扰,需使用基质匹配标准曲线校正,推荐采用同位素内标法提高准确性。
行业标准《蔬菜和水果中有机磷、有机氯、拟除虫菊酯和氨基甲酸酯类农药多残留检测方法》
标准名称及标准号NY/T 761-2004
适用范围适用于蔬菜、水果中高效氟吡甲禾灵及其他多类农药残留的筛查与定量。
核心检测方法气相色谱法(GC-ECD/NPD)或高效液相色谱法(HPLC)。
检出限与定量限高效氟吡甲禾灵的LOD为0.02 mg/kg,LOQ为0.1 mg/kg。
质控样品要求每批次至少10%的平行样,加标回收率应控制在80%-110%。
关键实验步骤1. 匀浆提取:丙酮-石油醚混合溶剂;2. 浓缩与溶剂置换;3. 色谱分离与检测。
特别说明该方法适用于高通量筛查,但对复杂基质需优化净化步骤,避免假阳性结果。
国家标准《实验室质量控制规范 食品理化检测》
标准名称及标准号GB/T 27404-2008
适用范围适用于所有食品检测实验室的质量控制,包括农药残留分析流程的规范性要求。
核心检测方法不涉及具体检测方法,规定人员资质、设备校准、方法验证等质控要求。
检出限与定量限要求实验室根据方法验证数据确定并记录LOD/LOQ,确保符合标准要求。
质控样品要求每批样品需包含空白对照、加标样品和平行样,数据保存至少6年。
关键实验步骤1. 方法确认:精密度、准确度、线性范围;2. 设备定期校准;3. 结果不确定度评估。
特别说明标准强调实验室需通过能力验证或比对实验证明检测能力,确保数据可靠性。

以上信息仅供参考,请以相应标准的原文为准!