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蒽_14938-35-3,4-戊基苯酚
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蒽介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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国家标准解读:蒽(CAS:14938-35-3)相关检测要求
标准名称及标准号 GB 11895-1989 《水质 苯并(a)芘的测定 乙酰化滤纸层析荧光分光光度法》
适用范围 适用于地表水、地下水及废水中多环芳烃(包括蒽)的痕量测定,检出限可达0.001 μg/L。
核心检测方法 水样经液-液萃取或固相萃取富集后,通过乙酰化滤纸层析分离目标物,荧光分光光度法定量分析蒽等组分。
检出限与定量限 检出限(LOD)为0.001 μg/L,定量限(LOQ)为0.003 μg/L,需通过校准曲线验证线性范围(通常为0.005-1.0 μg/L)。
质控样品要求 每批次样品须加标平行样(RSD≤15%),质控样品回收率需在80%-120%之间,空白实验值不得超过定量限的50%。
关键实验步骤 1. 样品酸化后用正己烷萃取;
2. 层析柱净化去除杂质;
3. 乙酰化滤纸分离多环芳烃;
4. 荧光检测器在激发波长365 nm、发射波长406 nm处定量。
特别说明 实验需避光操作以防止光解,蒽与其他多环芳烃共存时需优化色谱分离条件,必要时采用质谱法确认结构。

以上信息仅供参考,请以相应标准的原文为准!