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正十六烷_544-76-3,正十六烷
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正十六烷

BW901099-100mg {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 544-76-3 100mg {{goodObj.date}} 秦境 {{item.norm}} 99.0% {{inventory}}
正十六烷介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

n-Hexadecane

Product Code

BW901099

Lot Number

23081567

CAS No.

544-76-3

Mol. Formula

C16H34

Mol. Weight

226.44

Certified on

25 Aug 2023

Expiry Date

24 Aug 2028

Storage Temp

20°C ± 4°C

Specification

100mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.0%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external7 accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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标准名称及标准号
GB 17378.4-2007 《海洋监测规范 第4部分:海水分析》中"油类的测定 荧光分光光度法"
适用范围
适用于海水、沉积物及海洋生物体中石油类物质的测定,正十六烷作为标准物质用于建立标准曲线
核心检测方法
采用液液萃取-荧光分光光度法,正十六烷用于配制标准溶液并绘制荧光强度-浓度工作曲线
检出限与定量限
海水样品检出限0.002 mg/L,定量限0.006 mg/L;沉积物检出限2 mg/kg,定量限6 mg/kg
质控样品要求
每批次需带空白样和平行样,正十六烷标准溶液相对偏差应≤10%,标准曲线相关系数≥0.999
关键实验步骤
1. 正十六烷标准溶液梯度配制
2. 紫外激发波长310nm/发射波长360nm
3. 萃取剂需经正十六烷空白检验
特别说明
正十六烷标准溶液需避光冷藏保存,开封后有效期30天,使用前需进行纯度验证(色谱纯度≥98%)

以上信息仅供参考,请以相应标准的原文为准!