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3-硝基氯苯_
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3-硝基氯苯

BW901132 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 500mg {{goodObj.date}} 秦境 {{item.norm}} 99.5% {{inventory}}
3-硝基氯苯介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

1-Chloro-3-nitrobenzene

Product Code

BW901132

Lot Number

23101512

CAS No.

121-73-3

Mol. Formula

C6H4ClNO2

Mol. Weight

157.55

Certified on

30 Oct 2023

Expiry Date

29 Oct 2028

Storage Temp

20°C ± 4°C

Specification

500mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.5%

1.0%

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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国家标准:水质 硝基苯类化合物的测定 气相色谱法(GB 11889-1989)
标准名称及标准号
标准名称水质 硝基苯类化合物的测定 气相色谱法
标准号GB 11889-1989
适用范围
适用对象水体中硝基苯类化合物(包括3-硝基氯苯)的定量分析
适用场景环境监测、工业废水及生活污水检测
核心检测方法
方法原理水样经液液萃取或固相萃取后,用气相色谱仪分离,氢火焰离子化检测器(FID)定量。
色谱条件毛细管色谱柱(如DB-5),程序升温,载气为高纯氮气。
检出限与定量限
检出限0.1 μg/L(水样体积为1 L时)
定量限0.3 μg/L
质控样品要求
空白试验每批次需做空白样,结果应低于检出限
加标回收率80%-120%范围内为合格
平行样偏差≤15%
关键实验步骤
1. 样品预处理水样需用二氯甲烷萃取2次,合并萃取液后氮吹浓缩至1 mL。
2. 仪器分析进样量1 μL,分流比10:1,升温程序为初始50℃保持2 min,以10℃/min升至250℃。
3. 数据计算通过标准曲线法,以峰面积外标法定量。
特别说明
干扰消除若水样含复杂基质,需增加硅胶或氧化铝柱净化步骤。
安全提示3-硝基氯苯为有毒物质,实验需在通风橱内操作,佩戴防护装备。
行业标准:土壤和沉积物 硝基芳烃类化合物的测定 气相色谱-质谱法(HJ 834-2017)
标准名称及标准号
标准名称土壤和沉积物 硝基芳烃类化合物的测定 气相色谱-质谱法
标准号HJ 834-2017
适用范围
适用对象土壤及沉积物中硝基芳烃类化合物(含3-硝基氯苯)的定性与定量分析
适用场景污染场地调查、固体废物检测
核心检测方法
方法原理样品经索氏提取或加压流体萃取后净化,GC-MS分离检测。
质谱条件电离方式为EI源,扫描模式为SIM或全扫描。
质控样品要求
空白试验每20个样品需设置1个空白
基质加标加标回收率应满足60%-130%

以上信息仅供参考,请以相应标准的原文为准!