克百威
-
丙酮中克百威(呋喃丹)溶液
BW06127 | 100μg/mL
-
甲醇中呋喃丹(克百威)溶液标准物质
GBW(E)084547 | 1000μg/mL
-
甲醇中呋喃丹(克百威)溶液标准物质
GBW(E)084546 | 100μg/mL
-
丙酮中克百威(呋喃丹)溶液
BW06926 | 1000μg/mL
-
乙腈中克百威
BW-NCL-HB-00037 | 100μg/mL
-
甲醇中克百威
BW10222-1.2ml | 100μg/ml in methanol
-
甲醇中克百威
BW10223-1.2ml | 1000μg/ml in methanol
-
甲醇中强力霉素
BW-SCL-TM-00041 | 1000 mg/L
-
甲醇中金霉素
BW-SCL-TM-00040 | 1000 mg/L
-
甲醇中四环素
BW-SCL-TM-00263 | 1000μg/mL
-
甲醇中三聚氰胺
BW-OTL-HM-01554 | 100μg/mL
-
正己烷中4,4’-滴滴滴
BW-NCL-HN-00023 | 100μg/mL



Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.
Product Name
Carbofuran
Product Code
BW902017
Lot Number
23051518
CAS No.
1563-66-2
Mol. Formula
C12H15NO3
Mol. Weight
221.25
Certified on
26 May 2023
Expiry Date
25 May 2025
Storage Temp
20°C ± 4°C
Specification
100 mg
CERTIFIED
Purity
CERTIFIED
Expanded Uncertainty (U)
Approved by
98.6%
0.5%
Method of Characterisation
GC/FID
Batch Information
Water Content: <0.1% (by Karl-Fischer-Titration)
Uncertainty
The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.
The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.
Intended Use
This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.
Safety
Proper precautions should be observed while handling. See Safety Data Sheet.
Traceability
The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).
Homogeneity
Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.
Storage
The RM should be stored in the original sealed container at the indicated temperature.
Instructions for use
It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.
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标准号:GB 23200.113-2018
2. 仪器条件:高效液相色谱仪(HPLC)配备紫外检测器或二极管阵列检测器(DAD)。
3. 色谱条件:C18色谱柱(250 mm×4.6 mm, 5 μm),流动相为甲醇-水梯度洗脱,流速1.0 mL/min,检测波长210 nm。
定量限(LOQ):0.01 mg/kg(以克百威计)。
2. 回收率范围要求为70%-120%。
3. 每20个样品中至少插入1个平行样,相对偏差≤20%。
2. 提取:加入乙腈超声提取15 min,离心后取上清液。
3. 净化:使用PSA或C18固相萃取柱净化,洗脱液氮吹浓缩后用甲醇复溶。
4. 上机分析:按设定色谱条件进样,外标法定量。
2. 需关注流动相的脱气及色谱柱平衡时间(≥30 min)。
3. 当样品基质复杂时,建议使用质谱法(LC-MS/MS)进行确证。
以上信息仅供参考,请以相应标准的原文为准!