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1,2-二氯苯_95-50-1,1,2- 二氯苯
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1,2-二氯苯

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1,2-二氯苯介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.Uncertainty

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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标准名称及标准号
国家标准 GB/T 5750.8-2006《生活饮用水标准检验方法 有机物指标》
适用范围
适用于生活饮用水及其水源水中1,2-二氯苯的检测,覆盖水样前处理、仪器分析及结果计算全流程。
核心检测方法
气相色谱法(GC-ECD或GC-FID)。采用液液萃取或吹扫捕集技术进行前处理,使用色谱柱分离后定量分析。
检出限与定量限
方法检出限为0.5 μg/L,定量限为1.0 μg/L。需通过标准曲线校正,线性范围1-100 μg/L。
质控样品要求
每批次样品需包含空白对照、加标回收样和平行样。加标回收率应控制在80%-120%,相对标准偏差(RSD)≤15%。
关键实验步骤
1. 水样采集后需冷藏避光保存,7天内完成前处理;
2. 液液萃取使用正己烷或二氯甲烷提取;
3. 气相色谱条件:毛细管柱(30 m×0.32 mm×1.8 μm),柱温程序升温,进样口温度≥200℃,检测器温度≥250℃。
特别说明
1,2-二氯苯易挥发,实验过程需密闭操作;若样品含悬浮物需过滤或离心后分析。高浓度样品可能干扰结果,需稀释至线性范围内。

以上信息仅供参考,请以相应标准的原文为准!