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邻苯二甲酸二丁酯_84-74-2,邻苯二甲酸二丁酯
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邻苯二甲酸二丁酯

BW903046 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 84-74-2 500mg {{goodObj.date}} 秦境 {{item.norm}} 99.5% {{inventory}}
邻苯二甲酸二丁酯介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external7 accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Reference Material Producer:Shaanxi Qinjing Reference Material Science and Technology Center

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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1. 标准名称及标准号
GB/T 21911-2008《食品中邻苯二甲酸酯的测定》
2. 适用范围
适用于食品、食品添加剂及包装材料中邻苯二甲酸二丁酯(DBP)等16种邻苯二甲酸酯类物质的定性与定量分析。
3. 核心检测方法
气相色谱-质谱联用法(GC-MS),采用选择离子监测模式(SIM),通过保留时间和特征离子丰度比定性,外标法定量。
4. 检出限与定量限
邻苯二甲酸二丁酯的检出限(LOD)为0.05 mg/kg,定量限(LOQ)为0.2 mg/kg。
5. 质控样品要求
每批次样品需设置空白对照、加标回收实验(加标浓度为0.2-5.0 mg/kg),平行样相对偏差应≤20%,回收率控制在70%-120%。
6. 关键实验步骤
1. 样品经正己烷超声提取;
2. 提取液经硅胶固相萃取柱净化;
3. 氮吹浓缩后定容至1 mL;
4. GC-MS进样分析(色谱柱:DB-5MS,程序升温);
5. 数据分析与结果计算。
7. 特别说明
实验过程需严格避免塑料器具接触样品,防止人为引入污染。若检测值接近定量限,建议采用同位素内标法(如D4-DBP)进行确证。

以上信息仅供参考,请以相应标准的原文为准!