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灭多威_16752-77-5,灭多威
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灭多威

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灭多威介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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国家标准解读:灭多威(CAS:16752-77-5)相关检测标准
标准名称及标准号 GB 23200.113-2018 食品安全国家标准 植物源性食品中208种农药及其代谢物残留量的测定 液相色谱-质谱联用法
适用范围 适用于植物源性食品中灭多威及其他农药残留的定量检测,包括蔬菜、水果、谷物等基质。
核心检测方法 采用液相色谱-串联质谱法(LC-MS/MS),通过保留时间和特征离子对定性,外标法定量。
检出限与定量限 灭多威的检出限(LOD)为0.005 mg/kg,定量限(LOQ)为0.01 mg/kg。
质控样品要求 每批次样品需包含空白基质加标样品(添加浓度0.01-0.1 mg/kg),回收率应控制在70%-120%,相对标准偏差(RSD)≤20%。
关键实验步骤 1. 样品前处理:乙腈提取,QuEChERS法净化;
2. 仪器条件:C18色谱柱,流动相为0.1%甲酸水溶液和乙腈;
3. 质谱参数:多反应监测模式(MRM),母离子m/z 163.1,子离子m/z 88.1和106.1。
特别说明 灭多威易水解,样品提取后需在24小时内完成检测;基质效应需通过空白基质匹配校准曲线进行补偿。
其他相关行业标准参考
标准名称及标准号 GB 2763-2021 食品安全国家标准 食品中农药最大残留限量
关联内容 规定灭多威在各类食品中的最大残留限量(如谷物中限量为0.02 mg/kg),检测结果需符合该标准要求。

以上信息仅供参考,请以相应标准的原文为准!