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百里酚_89-83-8
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百里酚

BW905020 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 89-83-8 100mg {{goodObj.date}} 秦境 {{item.norm}} 99.6% {{inventory}}
百里酚介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

Thymol

Product Code

BW905020

Lot Number

23071537

CAS No.

89-83-8

Mol. Formula

C10H14O

Mol. Weight

150.22

Certified on

21 Jul 2023

Expiry Date

20 Jul 2028

Storage Temp

20°C ± 4°C

Specification

100mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.6%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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标准名称及标准号
标准名称 食品安全国家标准 食品中百里酚残留量的测定 气相色谱-质谱法
标准号 GB 23200.113-2018
适用范围
本标准适用于食品(包括植物源性食品、动物源性食品等)中百里酚残留量的检测,适用于进出口产品及国内食品监管领域。
核心检测方法
气相色谱-质谱联用法(GC-MS)。前处理包括样品粉碎、乙腈提取、弗罗里硅土柱净化、氮吹浓缩等步骤,最终通过色谱柱分离与质谱检测定量分析。
检出限与定量限
检出限 0.005 mg/kg
定量限 0.01 mg/kg
质控样品要求
每批次样品需包括空白样品、加标空白样品(低、中、高浓度)及实际样品平行分析。加标回收率应为70%-120%,相对标准偏差(RSD)≤15%。
关键实验步骤
1. 样品提取:使用乙腈超声辅助提取;
2. 净化:弗罗里硅土柱去除干扰物质;
3. 氮吹浓缩:40℃下氮吹至近干;
4. 仪器条件:DB-5MS色谱柱,升温程序80℃保持1min,以20℃/min升至260℃保持5min。
5. 质谱检测:选择离子监测(SIM)模式,定量离子为m/z 135。
特别说明
1. 需注意样品中酚类物质的干扰,必要时增加双波长检测;
2. 实验室环境温湿度需控制,避免有机溶剂挥发影响定量准确性;
3. 标准溶液需现配现用,避光保存不超过24小时。

以上信息仅供参考,请以相应标准的原文为准!