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乐果

BW902022 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 60-51-5 10mg {{goodObj.date}} 秦境 {{item.norm}} 98.5% {{inventory}}
乐果介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Dimethoate

Product Code

BW902022

Lot Number

25041513

CAS No.

60-51-5

Mol. Formula

C5H12NO3PS2

Mol. Weight

229.26

Certified on

9 Apr. 2025

Expiry Date

8 Apr. 2030

Storage Temp

-18°C ± 5°C

Specification

10mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

98.5%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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标准匹配结果
GB 23200.113-2018 食品安全国家标准 植物源性食品中208种农药及其代谢物残留量的测定
标准名称及标准号
GB 23200.113-2018 气相色谱-质谱联用法检测乐果等208种农药残留的核心标准
适用范围
适用于水果、蔬菜及谷物中乐果的定量分析,基质覆盖叶菜类、根茎类和浆果类
核心检测方法
气相色谱-质谱法(GC-MS) 配备电子轰击电离源(EI),采用选择离子监测(SIM)模式,乐果特征离子为87/125/229
检出限与定量限
方法检出限(LOD) 0.005 mg/kg(以样品基质计)
定量限(LOQ) 0.01 mg/kg
质控样品要求
空白加标回收率 70%-120%(添加浓度需≥LOQ)
平行样偏差 ≤20%(低浓度) / ≤15%(高浓度)
关键实验步骤
样品前处理 乙腈震荡提取→QuEChERS净化→氮吹浓缩定容
色谱条件 DB-5MS色谱柱(30m×0.25mm×0.25μm),进样口温度250℃,程序升温梯度
特别说明
1. 标准要求检测器响应值需≥3倍信噪比
2. 需定期进行基质效应验证试验
3. 建议每12小时重新校准仪器
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以上信息仅供参考,请以相应标准的原文为准!