o,p'-DDT
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丙酮中o,p'-DDT溶液标准物质(o,p'-滴滴涕)
BW03024 | 100μg/mL
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正己烷中o,p’-DDT溶液标准物质(o,p'-滴滴涕)
BW03023 | 100μg/mL
-
2,4-D
BW902040 | 98.9%
-
o,p'-DDE
BW902045 | 99.3%
-
异辛烷中o,p'-DDT
BW990018 | 100ug/mL
-
D-木糖
RMT13600 | 99.6%
-
2,4-D
| 见证书
-
甲醇中强力霉素
BW-SCL-TM-00041 | 1000 mg/L
-
甲醇中金霉素
BW-SCL-TM-00040 | 1000 mg/L
-
甲醇中四环素
BW-SCL-TM-00263 | 1000μg/mL
-
甲醇中三聚氰胺
BW-OTL-HM-01554 | 100μg/mL
-
正己烷中4,4’-滴滴滴
BW-NCL-HN-00023 | 100μg/mL



REFERENCE MATERIAL CERTIFICATE
Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.
Product Name
O,P’-DDT
Product Code
BW902044
Lot Number
23091505
CAS No.
789-02-6
Mol. Formula
C14H9Cl5
Mol. Weight
354.49
Certified on
2 Sep 2023
Expiry Date
1 Sep 2028
Storage Temp
20°C ± 4°C
Specification
10mg
CERTIFIED
Purity
CERTIFIED
Expanded Uncertainty (U)
Approved by
97.6%
1.0%
Method of Characterisation
GC/FID
Batch Information
Water Content: <0.1% (by Karl-Fischer-Titration)
Uncertainty
The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.
The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.
Intended Use
This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.
Safety
Proper precautions should be observed while handling. See Safety Data Sheet.
Traceability
The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).
Homogeneity
Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.
Storage
The RM should be stored in the original sealed container at the indicated temperature.
Instructions for use
It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.
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2. 气相色谱-质谱联用(GC-MS)分析
3. 采用选择离子监测模式(SIM)进行定量
定量限(LOQ):0.01 mg/kg(以样品干重计)
2. 加标浓度应覆盖定量限至10倍定量限范围
3. 回收率要求:70%-120%,相对标准偏差(RSD)≤15%
2. 加入乙腈震荡提取,离心分层
3. 取上清液经PSA和C18吸附剂净化
4. 氮吹浓缩后定容,GC-MS进样分析
2. 实验过程中需严格避免塑料器皿污染
3. 色谱柱推荐使用DB-5MS(30 m×0.25 mm×0.25 μm)
4. 方法验证需符合GB/T 27404-2008要求
以上信息仅供参考,请以相应标准的原文为准!