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吡啶

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吡啶介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Pyridine

Product Code

BW901109

Lot Number

25091510

CAS No.

110-86-1

Mol. Formula

C5H5N

Mol. Weight

79.10

Certified on

17 Sep. 2025

Expiry Date

16 Sep. 2030

Storage Temp

20°C ± 4°C

Specification

1g

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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1. 标准名称及标准号
GB/T 5750.8-2023《生活饮用水标准检验方法 第8部分:有机物指标》
2. 适用范围
适用于生活饮用水、水源水中吡啶的测定,检测浓度范围为0.05 mg/L~2.0 mg/L。
3. 核心检测方法
气相色谱法(GC-FID),通过色谱柱分离目标物,采用氢火焰离子化检测器定量分析。
4. 检出限与定量限
方法检出限(MDL)为0.02 mg/L,定量限(LOQ)为0.05 mg/L。
5. 质控样品要求
每批样品需包含至少1个空白样品、1个平行样及1个加标回收样,加标回收率应为80%~120%。
6. 关键实验步骤
(1)样品预处理:调节水样pH至碱性,用二氯甲烷萃取;
(2)色谱条件:DB-5毛细管柱(30 m×0.32 mm×0.25 μm),进样口温度250℃,检测器温度300℃;
(3)定量分析:外标法绘制标准曲线。
7. 特别说明
吡啶易挥发且有毒性,实验需在通风橱内操作;二氯甲烷废液需按危险废物处理。

以上信息仅供参考,请以相应标准的原文为准!