4 Organophosphate Insecticide Mix Solution in Acetonitrile, 1000μg/mL
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8 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST025401-100A | 1mL
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11 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST024549-100A | 1mL
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14 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST024428-100A | 1mL
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11 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST023683-100A | 1mL
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13 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST023073-100A | 1mL
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6 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST020855-100A | 1mL
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15 Organophosphate Insecticide Mix Solution in Acetonitrile, 100μg/mL
1ST020994-100A | 1mL
您正在浏览的产品:乙腈中4种有机磷杀虫剂混标溶液(HJ 1183-2021),1000μg/mL
手机版:乙腈中4种有机磷杀虫剂混标溶液(HJ 1183-2021),1000μg/mL
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1. 色谱条件:DB-5MS毛细管色谱柱(30m×0.25mm×0.25μm),程序升温(初始60℃保持1min,以20℃/min升至150℃,再以5℃/min升至280℃保持5min)
2. 质谱条件:电子轰击源(EI),选择离子监测模式(SIM),离子源温度230℃
3. 样品前处理:水样经0.45μm滤膜过滤后,用二氯甲烷或正己烷液液萃取
2. 平行样:每批样品至少10%平行双样,相对偏差≤20%
3. 加标回收:每批样品至少10%加标样,回收率70%~130%
4. 标准曲线:相关系数r≥0.995,每24小时需重新校准
2. 浓缩定容:合并萃取液经无水硫酸钠脱水,氮吹浓缩至0.5mL,用乙腈定容至1.0mL
3. 标准溶液配制:用乙腈稀释1000μg/mL混标溶液,配制5~100μg/L系列标准溶液
4. 上机分析:按标准色谱条件进样1μL,目标物响应值需在仪器线性范围内
2. 基质干扰消除:高基质样品需增加净化步骤(如弗罗里硅土柱)
3. 仪器维护:每批样品后需高温烘烤色谱柱(300℃保持30min)
4. 方法特异性:需监测各目标物特征离子比例(±30%内)
以上信息仅供参考,请以相应标准的原文为准!