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香豆素_91-64-5
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香豆素

BW903033 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 91-64-5 100mg {{goodObj.date}} 秦境 {{item.norm}} 98.2% {{inventory}}
香豆素介绍:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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国家标准: 食品安全国家标准 食品中香豆素的测定
标准名称及标准号 GB 5009.34-2022 食品安全国家标准 食品中香豆素的测定
适用范围 适用于食品(如饮料、糕点、调味品等)中香豆素含量的测定,检测限范围为0.01 mg/kg~10 mg/kg。
核心检测方法 高效液相色谱-荧光检测法(HPLC-FLD),以乙腈-水为流动相,C18色谱柱分离,激发波长280 nm,发射波长450 nm。
检出限与定量限 方法检出限(LOD)为0.005 mg/kg,定量限(LOQ)为0.015 mg/kg。
质控样品要求 每批次样品需加标平行样,回收率应控制在80%~120%;空白试验中不得检出目标物。
关键实验步骤 1. 样品经乙腈超声提取;
2. 提取液过0.22 μm滤膜;
3. 进样量10 μL,柱温30℃;
4. 外标法定量。
特别说明 避免使用含香豆素的本底污染容器;荧光检测器需定期校准;样品需避光保存。
行业标准: 进出口化妆品中香豆素的测定
标准名称及标准号 SN/T 5357-2021 进出口化妆品中香豆素的测定
适用范围 适用于膏霜、乳液、香水等化妆品中香豆素的检测,定量限为0.5 mg/kg。
核心检测方法 气相色谱-质谱联用法(GC-MS),DB-5MS色谱柱,程序升温,选择离子监测模式(SIM)。
质控样品要求 每批次样品需包含1个空白对照及2个加标平行样,相对标准偏差(RSD)应≤10%。

以上信息仅供参考,请以相应标准的原文为准!