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乙二醇二甲醚_110-71-4,1,2-二甲氧基乙烷
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乙二醇二甲醚

BW903004 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 110-71-4 0.5mL {{goodObj.date}} 秦境 {{item.norm}} 99.5% {{inventory}}
乙二醇二甲醚介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

1,2-Dimethoxyethane

Product Code

BW903004

Lot Number

23041540

CAS No.

110-71-4

Mol. Formula

C4H10O2

Mol. Weight

90.12

Certified on

20 Apr 2023

Expiry Date

19 Apr 2025

Storage Temp

20°C ± 4°C

Specification

0.5 mL

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.5%

0.5%

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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标准名称及标准号
GB/T 23972-2009
工业用乙二醇二甲醚纯度的测定 气相色谱法
适用范围
工业用乙二醇二甲醚及其他类似结构醚类化合物的纯度分析,适用于生产质量控制及产品验收。
核心检测方法
气相色谱法(GC-FID)
采用毛细管色谱柱分离,氢火焰离子化检测器(FID)定量分析,内标法计算主成分及杂质含量。
检出限与定量限
检出限(LOD) 0.001% (w/w)
定量限(LOQ) 0.003% (w/w)
质控样品要求
质控类型 平行样测试
内标物要求 选择与目标物无干扰、保留时间相近的内标物(如正庚烷)。
关键实验步骤
色谱条件设置 柱温程序:初始50℃保持2min,以10℃/min升至150℃,保持5min。
样品处理 准确称取样品并与内标物混合,稀释至适当浓度后进样分析。
特别说明
系统适用性 需确保色谱柱分离度(R≥1.5)及理论塔板数满足要求。

以上信息仅供参考,请以相应标准的原文为准!