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丁草胺_23184-66-9,丁草胺
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丁草胺

BW902011 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 23184-66-9 100mg {{goodObj.date}} 秦境 {{item.norm}} 94.9% {{inventory}}
丁草胺介绍:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

Butachlor

Product Code

BW902011

Lot Number

23051512

CAS No.

23184-66-9

Mol. Formula

C17H26ClNO2

Mol. Weight

311.85

Certified on

26 May 2023

Expiry Date

25May 2025

Storage Temp

4°C ± 4°C

Specification

100 mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

94.9%

0.5%

Method of Characterisation

GC/FID

Batch Information

Water Content: 0.1757% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values arebased on real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development for analyticaltechniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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标准名称及标准号
国家标准:GB 23200.113-2018 食品安全国家标准 植物源性食品中丁草胺等208种农药及其代谢物残留量的测定 液相色谱-质谱联用法
适用范围
适用于谷物、蔬菜、水果等植物源性食品中丁草胺残留量的测定,定量限范围为0.01~0.05 mg/kg。
核心检测方法
采用乙腈提取目标物,通过分散固相萃取(QuEChERS)法净化,结合液相色谱-三重四极杆质谱仪(LC-MS/MS)进行定性定量分析。
检出限与定量限
丁草胺的检出限(LOD)为0.003 mg/kg,定量限(LOQ)为0.01 mg/kg,不同基质可能需验证后调整。
质控样品要求
需包含空白对照、加标回收样品和平行样;加标回收率需控制在70%~120%,相对标准偏差(RSD)应≤15%。
关键实验步骤
1. 样品粉碎后均质;2. 乙腈超声提取30分钟;3. 分散固相萃取净化(PSA和C18吸附剂);4. 离心后上清液过膜,LC-MS/MS分析。
特别说明
高脂样品需增加净化步骤;不同仪器参数需优化;方法不适用于动物源性食品;丁草胺可能与其他酰胺类农药产生干扰,需调整色谱条件。

以上信息仅供参考,请以相应标准的原文为准!