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乙二醇甲醚_109-86-4,乙二醇甲醚
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乙二醇甲醚

BW903006 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 109-86-4 0.5mL {{goodObj.date}} 秦境 {{item.norm}} 99.3% {{inventory}}
乙二醇甲醚介绍:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

2-Methoxyethanol

Product Code

BW903006

Lot Number

23041542

CAS No.

109-86-4

Mol. Formula

C3H8O2

Mol. Weight

76.09

Certified on

20 Apr 2023

Expiry Date

19 Apr 2025

Storage Temp

20°C ± 4°C

Specification

0.5 mL

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.3%

0.5%

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values arebased on real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

标准名称及标准号
GB/T 23230-2009《危险化学品中有机溶剂纯度的测定 气相色谱法》
适用范围
本标准适用于含乙二醇甲醚等有机溶剂的危险化学品中纯度及杂质含量的测定,涵盖工业品、试剂的检测。
核心检测方法
采用毛细管柱气相色谱法,色谱柱建议使用DB-624或等效极性柱,载气为高纯氮气,检测器选用FID氢火焰离子化检测器。
检出限与定量限
乙二醇甲醚的仪器检出限(LOD)为0.05mg/L,方法定量限(LOQ)为0.15mg/L,需通过标准曲线法验证线性范围。
质控样品要求
每批次样品需包含空白对照、平行样和加标回收样,加标浓度应为待测物浓度的0.5-2倍,回收率需控制在85-115%。
关键实验步骤
1. 样品前处理:采用直接进样法,经0.22μm有机系滤膜过滤
2. 色谱条件:进样口温度250℃,检测器温度300℃,柱温程序升温50℃(2min)→20℃/min→220℃(5min)
3. 定性定量:通过保留时间定性,峰面积外标法定量
特别说明
1. 乙二醇甲醚易吸湿,样品需密封保存
2. 实验过程需在通风橱操作,避免接触皮肤
3. 当样品中含水率>1%时需采用脱水前处理

以上信息仅供参考,请以相应标准的原文为准!