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四氯化碳_56-23-5,四氯化碳
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四氯化碳

BW901002 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 56-23-5 0.5mL {{goodObj.date}} 秦境 {{item.norm}} 96.6% {{inventory}}
四氯化碳介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.Uncertainty

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Provin


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国家标准解读: 生活饮用水标准检验方法 第8部分:有机物指标(四氯化碳检测)
标准名称及标准号 GB/T 5750.8-2023 《生活饮用水标准检验方法 第8部分:有机物指标》
适用范围 适用于生活饮用水、水源水及水处理过程中四氯化碳的检测,覆盖液相微萃取-气相色谱法(GC-ECD)。
核心检测方法 气相色谱-电子捕获检测器法(GC-ECD),基于四氯化碳在色谱柱中分离后通过ECD检测器定量分析。
检出限与定量限 检出限为0.1 μg/L,定量限为0.3 μg/L;需通过标准曲线验证线性范围(0.3~50 μg/L)。
质控样品要求 每批次至少包含1个空白样、1个平行样和1个加标回收样,加标浓度需覆盖实际样品浓度范围(建议0.5~2倍定量限)。
关键实验步骤 1. 水样用正己烷萃取;
2. 无水硫酸钠脱水;
3. GC进样参数:色谱柱为DB-624(30 m×0.32 mm×1.8 μm),柱温程序初始60℃保持1 min,以10℃/min升温至200℃。
特别说明 四氯化碳为易挥发有毒物质,需在通风橱内操作;样品需4℃避光保存且24小时内完成前处理。
行业标准解读: 水质 挥发性有机物的测定 吹扫捕集/气相色谱-质谱法(四氯化碳检测)
适用范围 适用于地下水、地表水及废水中四氯化碳的检测,检测下限可低至0.03 μg/L。
核心检测方法 吹扫捕集与GC-MS联用技术,采用内标法定量(推荐内标物为溴氯甲烷)。
质控要求 校准曲线相关系数需≥0.995;连续分析时每10个样品插入校准空白检查。

以上信息仅供参考,请以相应标准的原文为准!