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萘-D8_1146-65-2,萘-D8
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萘-D8

BW908002 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 1146-65-2 100mg {{goodObj.date}} 秦境 {{item.norm}} 97.5% {{inventory}}
萘-D8介绍:

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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相关标准解读:萘-D8(CAS:1146-65-2)在环境检测中的应用
标准名称及标准号 HJ 647-2013 环境空气和废气 气相和颗粒物中多环芳烃的测定 气相色谱-质谱法》
适用范围 本标准适用于环境空气、固定污染源废气中16种多环芳烃(PAHs)及其衍生物的测定,萘-D8作为内标物用于定性和定量分析。
核心检测方法 采用气相色谱-质谱联用法(GC-MS),样品经索氏提取或超声萃取后净化,萘-D8作为内标加入以校正目标物回收率。
检出限与定量限 萘-D8作为内标时,方法对多环芳烃的检出限为0.05-0.5 μg/m³(气体)或0.1-1.0 ng/g(颗粒物),定量限为检出限的3倍。
质控样品要求 每批次样品需添加等量萘-D8内标(建议浓度1.0 μg/mL),平行样相对偏差≤20%,加标回收率需在60-120%范围内。
关键实验步骤 1. 样品前处理:滤膜/滤筒用正己烷-丙酮混合溶剂萃取
2. 内标添加:在萃取液中精确加入萘-D8溶液
3. 仪器分析:GC-MS分离后采用SIM模式检测
特别说明 萘-D8需在样品萃取后、浓缩前加入,避免因挥发性差异导致定量偏差;当样品中萘含量过高时需验证内标响应是否受抑制。

以上信息仅供参考,请以相应标准的原文为准!