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1-辛烯_111-66-0,1-辛烯
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1-辛烯

BW901005 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 111-66-0 0.5mL {{goodObj.date}} 秦境 {{item.norm}} 98.0% {{inventory}}
1-辛烯介绍:

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values are basedon real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal7 accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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标准名称及标准号
GB/T 18883-2022 室内空气质量标准
GBZ/T 160.40-2004 工作场所空气有毒物质测定 混合烃类化合物
适用范围
GB/T 18883-2022 适用于室内环境空气中挥发性有机化合物(包括1-辛烯)的限值要求及检测方法。
GBZ/T 160.40-2004 适用于职业卫生领域中对工作场所空气中1-辛烯等混合烃类化合物的采样及分析。
核心检测方法
GB/T 18883-2022 推荐使用气相色谱-质谱法(GC-MS)进行定性定量分析,并规定了热脱附进样技术要求。
GBZ/T 160.40-2004 规定了活性炭管采集、二硫化碳解吸后使用气相色谱法(GC-FID)进行检测的详细流程。
检出限与定量限
GB/T 18883-2022 中1-辛烯的方法检出限为0.5 μg/m³,定量限为1.5 μg/m³(基于采样体积10L)。
GBZ/T 160.40-2004 要求定量限不高于0.1 mg/m³,实际检出限取决于解吸效率和仪器灵敏度。
质控样品要求
两类标准均要求每批次检测包含空白对照样、平行样及加标回收样,加标回收率需控制在80%-120%之间。
关键实验步骤
1. 采样阶段需控制流量偏差≤5%,GBZ/T 160.40-2004明确规定活性炭管采样流速为0.5 L/min
2. 样品前处理需在规定时间内完成解吸(GBZ/T标准要求解吸后4小时内上机分析)
3. 气相色谱分析时需使用DB-1或等效色谱柱,柱温程序需按标准梯度设置
特别说明
1. GB/T 18883-2022 规定当1-辛烯与其他烯烃共存时需使用极性色谱柱辅助定性
2. 标准物质贮存时需避光保存于4℃以下,开封后需进行密封性验证

以上信息仅供参考,请以相应标准的原文为准!