• 欢迎来到萘析商城
对硫磷_56-38-2,对硫磷
图片仅供参考,具体产品以实物为准!

对硫磷

BW902046 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 56-38-2 100mg {{goodObj.date}} 秦境 {{item.norm}} 99.4% {{inventory}}
对硫磷介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Parathion-ethyl

Product Code

BW902046

Lot Number

23091507

CAS No.

56-38-2

Mol. Formula

C10H14NO5PS

Mol. Weight

291.26

Certified on

2 Sep 2023

Expiry Date

1 Sep 2026

Storage Temp

4°C ± 4°C

Specification

100mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.4%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


您正在浏览的产品:对硫磷

手机版:对硫磷

本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

标准名称及标准号
GB 23200.113-2018《食品安全国家标准 植物源性食品中多种农药残留量的测定》
适用范围
适用于植物源性食品(如蔬菜、水果、谷物等)中对硫磷等有机磷类农药残留量的测定。
核心检测方法
采用气相色谱-质谱联用法(GC-MS)进行定性和定量分析,样品经乙腈提取后,通过固相萃取柱净化处理。
检出限与定量限
对硫磷的检出限(LOD)为0.01 mg/kg,定量限(LOQ)为0.02 mg/kg。
质控样品要求
每批次样品需加入空白对照、空白加标样品及平行样,加标回收率应控制在70%-120%范围内。
关键实验步骤
1. 样品均质后,乙腈振荡提取;
2. 提取液经PSA固相萃取柱净化;
3. 氮吹浓缩至干,定容后进行GC-MS分析;
4. 采用外标法计算残留量。
特别说明
高脂类样品需增加石墨化碳黑(GCB)净化步骤,以避免基质干扰。实验需在通风橱内操作,佩戴防护装备。
标准名称及标准号
GB/T 5750.9-2022《生活饮用水标准检验方法 农药指标》
适用范围
适用于生活饮用水、水源水中对硫磷等有机磷农药的检测。
核心检测方法
使用气相色谱法(GC-FPD),水样经二氯甲烷液液萃取后分析,通过保留时间定性、峰面积定量。
检出限与定量限
对硫磷的检出限为0.0003 mg/L,定量限为0.001 mg/L。
质控样品要求
每10个样品需加入1个空白样和1个加标平行样,加标回收率需满足80%-110%。
关键实验步骤
1. 调节水样pH至中性;
2. 二氯甲烷分三次萃取,合并有机相;
3. 无水硫酸钠脱水后浓缩;
4. 进样分析并计算浓度。
特别说明
萃取过程需避光操作,浓缩温度不得超过40℃。若水样含悬浮物需预先过滤。

以上信息仅供参考,请以相应标准的原文为准!