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正丁醇_
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正丁醇

BW901112 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 1g {{goodObj.date}} 秦境 {{item.norm}} 99.7% {{inventory}}
正丁醇介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

1-Butanol

Product Code

BW901112

Lot Number

23091522

CAS No.

71-36-3

Mol. Formula

C4H10O

Mol. Weight

74.12

Certified on

13 Sep 2023

Expiry Date

12 Sep 2028

Storage Temp

20°C ± 4°C

Specification

1g

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.7%

1.0%

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

1. 标准名称及标准号
《工业用正丁醇》GB/T 339-2019
2. 适用范围
适用于以羰基合成法或发酵法制得的工业用正丁醇的质量控制,包括纯度、水分、酸度及其他杂质含量的检测。
3. 核心检测方法
气相色谱法(GC):通过色谱柱分离正丁醇与其他组分,氢火焰离子化检测器(FID)定量分析主组分及杂质含量。
4. 检出限与定量限
杂质组分(如异丁醇、仲丁醇)检出限≤0.005%(质量分数),定量限≤0.01%(质量分数);水分(卡尔·费休法)定量限≤0.02%。
5. 质控样品要求
每批次样品需包含平行样,平行测定差值应小于0.05%;使用有证标准物质或加标回收实验验证,回收率需在95%-105%范围内。
6. 关键实验步骤
样品预处理:取1μL液体样品直接进样,无需稀释;色谱条件:毛细管柱(如HP-INNOWAX),柱温程序从60℃升至200℃,载气为高纯氮气,流速1.0 mL/min。
7. 特别说明
若样品含高沸点杂质需提高终温至240℃并延长保留时间;实验人员需佩戴防毒面具,正丁醇为易燃液体,需远离火源。

以上信息仅供参考,请以相应标准的原文为准!