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正丁醇_
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正丁醇

BW901112 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 500mg {{goodObj.date}} 秦境 {{item.norm}} 99.7% {{inventory}}
正丁醇介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

1-Butanol

Product Code

BW901112

Lot Number

23091523

CAS No.

71-36-3

Mol. Formula

C4H10O

Mol. Weight

74.12

Certified on

13 Sep 2023

Expiry Date

12 Sep 2028

Storage Temp

20°C ± 4°C

Specification

500mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.7%

1.0%

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

1. 标准名称及标准号
GB/T 23990-2008
2. 适用范围
本标准适用于涂料、油墨及相关产品中正丁醇含量的测定,适用于溶剂型涂料及含有机溶剂的产品质量控制。
3. 核心检测方法
气相色谱法(GC-FID):通过色谱柱分离样品中正丁醇与其他组分,氢火焰离子化检测器(FID)定量分析。
4. 检出限与定量限
检出限(LOD)为0.5 mg/kg,定量限(LOQ)为2.0 mg/kg,适用于低浓度正丁醇的痕量检测。
5. 质控样品要求
每批次样品需包含空白对照、平行样及加标回收样,回收率范围应控制在85%-115%,相对标准偏差(RSD)≤5%。
6. 关键实验步骤
① 样品预处理:称取1.0 g样品,用丙酮萃取并过滤;
② 色谱条件:DB-WAX色谱柱,柱温120℃→220℃(10℃/min),进样量1 μL;
③ 校准曲线:配制0.5-50 mg/L正丁醇标准系列。
7. 特别说明
① 避免使用含醇类溶剂的实验耗材;
② 若样品含高沸点干扰物,需采用程序升温至280℃进行彻底洗脱;
③ 实验环境温度需控制在25±2℃。

以上信息仅供参考,请以相应标准的原文为准!