ASTM方法大全2/D5185（EN14105）_混标_基质类_标准物质_萘析商城

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ASTM方法大全2/D5185（EN14105）

D5185

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ASTM-02

VHG

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ASTM方法大全2/D5185介绍：

ASTM标准油方法大全2-描述
ASTM # Method Description	Cross Reference Tables (ASTM,IP,ISO,DIN,JIS,AFNOR)
D56	Flash Point by TAG Closed Cup
D86	Synthetic Distillation Standard
D92	Flash Point Standards (COC)
D93	Flash Point Standards (PMCC)
D445	Viscosity Calibration Standard
D611	Aniline Point Standard
D1015	Freezing Point Standards
D1319	Olefin Analysis by FIA
D1744	Water in Liquid Petroleum Products
D2386	Freezing Point Calibration Standards
D2500	Cloud Point Calibration Standards
D2622	Sulfur by XRF
D2789	PIANO, PONA, PNA by GC
Hydrocarbon Analysis in Gasoline by GC/MS
D2887	Boiling Range by GC
Simulated Distillation (SIM DIS) by GC
D3120	Sulfur by Oxidative Microcoulometry
D3230	Salts in Crude Oil
D3231	Phosphorus in Gasoline
D3237	Lead in Gasoline by AA
D3246	Sulfur in Petroleum Gas by Oxidative Microcoulometry
D3340	Li & Na in Lubricating Greases by Flame Photometer
D3524	Diesel Fuel Analysis by GC
D3605	Trace Metal in Gas Turbine Fuels by AA
D3606	Aromatics in Gasoline by GC
D3610	Total Co Analysis by Potentiometric Titration
D3710	Boiling Range by GC
D3798	p-Xylene Analysis by GC
D3831	Manganese in Gasoline by AA
D4059	PCB Analysis by GC
D4110	Ion Chrom
D4291	Ethylene Glycol by GC
D4294	Sulfur by ED-XRF
D4377	Water in Liquid Petroleum Products
D4420	Aromatics in Gasoline by GC
D4628	Wear Metals in Lube Oil
D4629	Nitrogen by Chemiluminescence
D4815	Oxygenates in Gasoline by GC
D4927	Wear Metals and Additives by WD-XRF
D4928	Water in Liquid Petroleum Products
D4929	Chlorine in Crude Oil by Microcoulometry
D4951	Wear Metals and Additives by ICP
D5056	Trace Metals in Petroleum Coke by AA
D5059	Lead in Gasoline by X-Ray Spectroscopy
D5134	Petroleum Naphthas through n-Nonane by GC
D5184	Al and Si by ICP-AES & AA
D5185	Wear Metals and Additives by ICP
D5186	Aromatics by SFC
D5188	Vapor - Liquid Ratio Temperature
D5191	Vapor Pressure Standards
D5307	Boiling Range Distribution of Crude Petroleum by GC
D5441	MtBE Analysis by GC
D5442	PetroleumWaxes by GC
D5443	PNA Analysis by Multidimensional GC
D5453	Sulfur by Ultra Violet Fluorescence
D5480	Engine Oil Volatility by GC
D5482	Vapor Pressure Standards
D5501	Ethanol Analysis by GC
D5580	Aromatics by GC
D5599	Oxygenates by OFID
D5600	Trace Metals by ICP
D5622	Oxygenates by Reductive Pyrolysis
D5623	Sulfur Compounds by Sulfur Selective Detection
D5708	Trace Metals by ICP
D5762	Nitrogen by Chemiluminescence
D5769	Aromatics by GC/MS
D5771	Cloud Point of Petro Products
D5772	Cloud Point of Petro Products (Linear Cooling Rate)
D5773	Cloud Point of Petro Products (Constant Cooling Rate)
D5836	Diisocyanates
D5863	Trace Metals by AA
D5901	Freezing Point Aviation Fuels (Auto Optical Method)
D5972	Freezing Point Aviation Fuels
D5986	Oxygenates and Aromatics by GC/FTIR
D6042	Plastic Packaging Testing
D6160	PCBs by GC
D6258	Solvent Red 164 Dye Concentration in Diesel Fuels
D6277	Benzene in Spark Ignition Fuels
D6293	Oxygenates (O-PONA) in Engine Fuels by GC
D6296	Total Olefins in Spark Ignition Engine Fuels by GC
D6304	Water in Liquid Petro Products
D6334	Sulfur in Gasoline byWavelength WD-XRF
D6352	Boiling Range Distribution of Petroleum
D6378	Vapor Pressure
D6379	Aromatic Hydrocarbon by HPLC
D6417	Engine Oil by GC
D6428	Sulfur by ECD
D6443	Metals in Oil
D6445	Sulfur in Gasoline by ED-XRF
D6481	Lube Oils by ED-XRF
D6550	Olefin Content of Gasoline by SFC
D6584	(EN14105) Free and Total Glycerin
D6591	(IP 391) Aromatic Hydrocarbon by HPLC
D6751	Sulfur in Biodiesel
D7065	Nonylphenol and Octylphenol
E1064	Water in Petroleum
E1387	Fire Debris Analysis
E1618	Fire Debris Analysis
Sulfur Standards Group
D2622	Sulfur by XRF
D3120	Sulfur by Oxidative Microcoulometry
D3246	Sulfur in Petro Gas by Oxidative Microcoulometry
D4294	Sulfur by ED-XRF
D5453	Sulfur by Ultra Violet Fluorescence
D5623	Sulfur Compounds by Sulfur Selective Detection
D6334	Sulfur in Gasoline byWavelength WD-XRF
D6445	Sulfur in Gasoline by ED-XRF
Wear Metals Group
D3605	Trace Metals in Gas Turbine Fuel by AA
D4628	Wear Metals in Lube Oil
D4927	Wear Metals and Additives by WDXRF
D4951	Wear Metals and Additives by ICP
D5185	Wear Metals and Additives by ICP
D5708	Trace Metals by ICP
D5863	Trace Metals by AA
D6443	Metals in Oil
D6481	Lube Oils by ED-XRF
Additional Methods
Motor Oil Standards
Method 1664, Oil, Grease & TPH Analysis
Methods 413.2, 418.1 & TPH Analysis
Method 8440 TPH Analysis
Method 1004 Alcohol Oxidation Products in Engine Exhaust

ASTM Methods
ASTM # Method Description	Cross Reference Tables (ASTM,IP,ISO,DIN,JIS,AFNOR)
D56	Flash Point by TAG Closed Cup
D86	Synthetic Distillation Standard
D92	Flash Point Standards (COC)
D93	Flash Point Standards (PMCC)
D445	Viscosity Calibration Standard
D611	Aniline Point Standard
D1015	Freezing Point Standards
D1319	Olefin Analysis by FIA
D1744	Water in Liquid Petroleum Products
D2386	Freezing Point Calibration Standards
D2500	Cloud Point Calibration Standards
D2622	Sulfur by XRF
D2789	PIANO, PONA, PNA by GC
Hydrocarbon Analysis in Gasoline by GC/MS
D2887	Boiling Range by GC
Simulated Distillation (SIM DIS) by GC
D3120	Sulfur by Oxidative Microcoulometry
D3230	Salts in Crude Oil
D3231	Phosphorus in Gasoline
D3237	Lead in Gasoline by AA
D3246	Sulfur in Petroleum Gas by Oxidative Microcoulometry
D3340	Li & Na in Lubricating Greases by Flame Photometer
D3524	Diesel Fuel Analysis by GC
D3605	Trace Metal in Gas Turbine Fuels by AA
D3606	Aromatics in Gasoline by GC
D3610	Total Co Analysis by Potentiometric Titration
D3710	Boiling Range by GC
D3798	p-Xylene Analysis by GC
D3831	Manganese in Gasoline by AA
D4059	PCB Analysis by GC
D4110	Ion Chrom
D4291	Ethylene Glycol by GC
D4294	Sulfur by ED-XRF
D4377	Water in Liquid Petroleum Products
D4420	Aromatics in Gasoline by GC
D4628	Wear Metals in Lube Oil
D4629	Nitrogen by Chemiluminescence
D4815	Oxygenates in Gasoline by GC
D4927	Wear Metals and Additives by WD-XRF
D4928	Water in Liquid Petroleum Products
D4929	Chlorine in Crude Oil by Microcoulometry
D4951	Wear Metals and Additives by ICP
D5056	Trace Metals in Petroleum Coke by AA
D5059	Lead in Gasoline by X-Ray Spectroscopy
D5134	Petroleum Naphthas through n-Nonane by GC
D5184	Al and Si by ICP-AES & AA
D5185	Wear Metals and Additives by ICP
D5186	Aromatics by SFC
D5188	Vapor - Liquid Ratio Temperature
D5191	Vapor Pressure Standards
D5307	Boiling Range Distribution of Crude Petroleum by GC
D5441	MtBE Analysis by GC
D5442	PetroleumWaxes by GC
D5443	PNA Analysis by Multidimensional GC
D5453	Sulfur by Ultra Violet Fluorescence
D5480	Engine Oil Volatility by GC
D5482	Vapor Pressure Standards
D5501	Ethanol Analysis by GC
D5580	Aromatics by GC
D5599	Oxygenates by OFID
D5600	Trace Metals by ICP
D5622	Oxygenates by Reductive Pyrolysis
D5623	Sulfur Compounds by Sulfur Selective Detection
D5708	Trace Metals by ICP
D5762	Nitrogen by Chemiluminescence
D5769	Aromatics by GC/MS
D5771	Cloud Point of Petro Products
D5772	Cloud Point of Petro Products (Linear Cooling Rate)
D5773	Cloud Point of Petro Products (Constant Cooling Rate)
D5836	Diisocyanates
D5863	Trace Metals by AA
D5901	Freezing Point Aviation Fuels (Auto Optical Method)
D5972	Freezing Point Aviation Fuels
D5986	Oxygenates and Aromatics by GC/FTIR
D6042	Plastic Packaging Testing
D6160	PCBs by GC
D6258	Solvent Red 164 Dye Concentration in Diesel Fuels
D6277	Benzene in Spark Ignition Fuels
D6293	Oxygenates (O-PONA) in Engine Fuels by GC
D6296	Total Olefins in Spark Ignition Engine Fuels by GC
D6304	Water in Liquid Petro Products
D6334	Sulfur in Gasoline byWavelength WD-XRF
D6352	Boiling Range Distribution of Petroleum
D6378	Vapor Pressure
D6379	Aromatic Hydrocarbon by HPLC
D6417	Engine Oil by GC
D6428	Sulfur by ECD
D6443	Metals in Oil
D6445	Sulfur in Gasoline by ED-XRF
D6481	Lube Oils by ED-XRF
D6550	Olefin Content of Gasoline by SFC
D6584	(EN14105) Free and Total Glycerin
D6591	(IP 391) Aromatic Hydrocarbon by HPLC
D6751	Sulfur in Biodiesel
D7065	Nonylphenol and Octylphenol
E1064	Water in Petroleum
E1387	Fire Debris Analysis
E1618	Fire Debris Analysis
Sulfur Standards Group
D2622	Sulfur by XRF
D3120	Sulfur by Oxidative Microcoulometry
D3246	Sulfur in Petro Gas by Oxidative Microcoulometry
D4294	Sulfur by ED-XRF
D5453	Sulfur by Ultra Violet Fluorescence
D5623	Sulfur Compounds by Sulfur Selective Detection
D6334	Sulfur in Gasoline byWavelength WD-XRF
D6445	Sulfur in Gasoline by ED-XRF
Wear Metals Group
D3605	Trace Metals in Gas Turbine Fuel by AA
D4628	Wear Metals in Lube Oil
D4927	Wear Metals and Additives by WDXRF
D4951	Wear Metals and Additives by ICP
D5185	Wear Metals and Additives by ICP
D5708	Trace Metals by ICP
D5863	Trace Metals by AA
D6443	Metals in Oil
D6481	Lube Oils by ED-XRF
Additional Methods
Motor Oil Standards
Method 1664, Oil, Grease & TPH Analysis
Methods 413.2, 418.1 & TPH Analysis
Method 8440 TPH Analysis
Method 1004 Alcohol Oxidation Products in Engine Exhaust

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GB/T 17476-2020 使用过的润滑油中添加剂元素、磨损金属和污染物以及基础油中某些元素的测定电感耦合等离子体发射光谱法

标准名称及标准号

GB/T 17476-2020（等效采用ASTM D5185）

适用范围

适用于测定使用过的润滑油中22种元素（Al、Sb、Ba、B、Ca、Cr、Cu、Fe、Pb、Mg、Mn、Mo、Ni、P、K、Na、Si、Ag、Sn、Sr、Ti、Zn）含量，检测范围0.1~1000 mg/kg

核心检测方法

电感耦合等离子体发射光谱法（ICP-OES），样品经有机溶剂稀释后直接进样分析

检出限与定量限

典型元素检出限0.01~0.5 mg/kg，定量限0.1~1.0 mg/kg（需根据仪器性能实际验证）

质控样品要求

每批样品需带空白、标准物质（CRM）及加标回收样：
1. 空白样品：基础油或溶剂空白
2. 标准物质：NIST SRM 1084a/1085a
3. 加标回收率：85%~115%

关键实验步骤

1. 样品制备：称取0.5g油样+10mL稀释剂（煤油/二甲苯）
2. 仪器校准：多元素混合标准溶液建立校准曲线
3. 分析条件：射频功率≥1.2kW，雾化气流量0.6~1.0 L/min
4. 干扰校正：需验证光谱干扰并选择最佳分析谱线

特别说明

1. 需验证元素间干扰（如Ba对Ti的谱线干扰）
2. 高粘度样品需增加稀释比例或加热处理
3. 结果需注明稀释因子（DF）计算方式

GB/T 36590-2018 生物柴油中游离甘油和总甘油含量的测定气相色谱法

标准名称及标准号

GB/T 36590-2018（技术等效EN 14105）

适用范围

适用于生物柴油（脂肪酸甲酯）中游离甘油（0.005%~0.07%）和总甘油（0.05%~0.7%）的含量测定

核心检测方法

气相色谱法（GC-FID）：
1. 游离甘油：样品直接衍生化后进样
2. 总甘油：经水解将甘油酯转化为游离甘油后衍生化

检出限与定量限

游离甘油定量限：0.005% (m/m)
总甘油定量限：0.02% (m/m)

质控样品要求

1. 每20个样品需带质控样（已知甘油含量）
2. 平行样相对偏差≤10%
3. 标准物质：NIST SRM 2772生物柴油

关键实验步骤

1. 衍生化：N-甲基-N-三甲基硅基三氟乙酰胺（MSTFA）
2. 色谱条件：DB-5ht色谱柱（15m×0.32mm×0.1μm）
3. 程序升温：50℃(1min)→15℃/min→180℃→40℃/min→380℃(5min)
4. 定量方法：内标法（1,2,3-丁三醇）

特别说明

1. 水解步骤需严格控温(75±5℃)和时间(15min)
2. 衍生化后须在8小时内完成检测
3. 需监控色谱柱惰性（甘油峰拖尾因子≤1.5）

以上信息仅供参考，请以相应标准的原文为准！