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氯氰菊酯_52315-07-8,氯氰菊酯
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氯氰菊酯

BW902010 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 52315-07-8 100mg {{goodObj.date}} 秦境 {{item.norm}} 95.8% {{inventory}}
氯氰菊酯介绍:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

Cypermethrin

Product Code

BW902010

Lot Number

23051511

CAS No.

52315-07-8

Mol. Formula

C22H19Cl2NO3

Mol. Weight

416.30

Certified on

26 May 2023

Expiry Date

25May 2025

Storage Temp

20°C ± 4°C

Specification

100 mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

95.8%

0.8%

Method of Characterisation

GC/FID

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values arebased on real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development foranalytical techniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by a factorof two for half sample and four for a quarter of sample. If storage afteropening is necessary, the RM should be tightly closed and kept from light andmoisture. If the RM was in a sealed ampoule, it should be transferred to a vialwith minimum head space.


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

国家标准解读:《食品安全国家标准 植物源性食品中氯氰菊酯残留量的测定》
标准名称及标准号GB 23200.113-2018《食品安全国家标准 植物源性食品中氯氰菊酯残留量的测定》
适用范围适用于蔬菜、水果、谷物等植物源性食品中氯氰菊酯及其异构体残留量的检测。
核心检测方法气相色谱-质谱联用法(GC-MS),采用内标法定量,通过提取、净化、浓缩等步骤测定目标物。
检出限与定量限检出限(LOD)为0.01 mg/kg,定量限(LOQ)为0.03 mg/kg,满足农残限量管控要求。
质控样品要求每批次样品需加标回收实验,空白样品中添加浓度应为LOQ的1~5倍,回收率需控制在70%~120%。
关键实验步骤1. 样品均质化后用乙腈提取;2. 通过固相萃取柱(SPE)净化;3. 氮吹浓缩至干后用丙酮复溶;4. 上机分析,保留时间和特征离子定性定量。
特别说明检测过程中需注意氯氰菊酯的同分异构体分离问题,建议使用毛细管色谱柱(如DB-5MS)优化分离条件。

以上信息仅供参考,请以相应标准的原文为准!