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乙酸正丙酯_109-60-4,乙酸丙酯
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乙酸正丙酯

BW901050 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 109-60-4 0.5mL {{goodObj.date}} 秦境 {{item.norm}} 99.5% {{inventory}}
乙酸正丙酯介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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以下是针对乙酸正丙酯(CAS:109-60-4)相关国家标准的解读:
标准名称及标准号
GB/T 23986-2009
涂料中挥发性有机化合物(VOC)含量的测定
适用范围
适用于涂料、油漆及相关产品中乙酸正丙酯等挥发性有机物的定量分析,包含溶剂型和水性涂料体系
核心检测方法
气相色谱法(GC-FID),采用内标法定量,色谱柱推荐使用DB-624等中等极性毛细管柱
检出限与定量限
检出限(LOD): 2.5 mg/kg
定量限(LOQ): 8.3 mg/kg
质控样品要求
1. 每批次样品需加测空白样、平行样及加标回收样
2. 加标浓度应为待测物浓度的50%-150%
3. 平行样相对偏差应≤15%
关键实验步骤
1. 样品前处理:称取0.5g样品,用甲醇/丙酮(1:1)混合溶剂超声提取
2. 色谱条件:进样口温度250℃,检测器温度300℃,柱温程序40℃→280℃
3. 系统适应性:连续进样3针RSD≤5%
特别说明
1. 乙酸正丙酯在高温下易分解,需严格控制热解析温度
2. 需注意与乙酸异丙酯的色谱分离(分离度≥1.5)
3. 标准物质应避光保存于4℃环境

以上信息仅供参考,请以相应标准的原文为准!