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3-硝基苯胺_99-09-2,3-硝基苯胺
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3-硝基苯胺

BW903029 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 99-09-2 500mg {{goodObj.date}} 秦境 {{item.norm}} 99.5% {{inventory}}
3-硝基苯胺介绍:

Reference Material

This certificate is designed in accordance with ISO17034 and ISO Guide 31. This reference material (RM) was designed,produced andverified in accordance with ISO/IEC 17025, ISO 17034 and a registered qualitymanagement system ISO9001.

Product Name

3-Nitroaniline

Product Code

BW903029

Lot Number

23061581

CAS No.

99-09-2

Mol. Formula

C6H6N2O2

Mol. Weight

138.12

Certified on

26 Jun 2023

Expiry Date

29 Jun 2028

Storage Temp

4°C ± 4°C

Specification

500mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.5%

1.0%

Methodof Characterisation

GC/FID

Batch Information

Water Content: <0.30% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) aredetermined in accordance with ISO 17034 with an 95% confidence level (k=2).Uncertainty is based on the Total Combined Uncertainty, including uncertaintiesof characterisation, homogeneity and stability testing. Stability values arebased on real evidence opposed to simulation.

The producer certifies that this reference materialmeets the specification stated in this certificate until the expiry date,provided it is stored unopened at the recommended temperature herein. Productwarranties for this reference material are set out in the terms and conditionsof purchase.

Intended Use

This RM is intended for use in a laboratory as acalibration and quality control standard or in method development for analyticaltechniques.

Safety

Proper precautions should be observed whilehandling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements arecalibrated with weights traceable to the national standards (DKD). Thecalibration of the balances is verified daily internally and annually by anexternal accredited calibration service. Chromatographic methods are traceableto the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RMhave been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealedcontainer at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum samplesize and if less material is used, to increase the certified uncertainty by afactor of two for half sample and four for a quarter of sample. If storageafter opening is necessary, the RM should be tightly closed and kept from lightand moisture. If the RM was in a sealed ampoule, it should be transferred to avial with minimum head space.


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标准名称及标准号
GB/T 5750.8-2023《生活饮用水标准检验方法 有机物指标》
适用范围
适用于生活饮用水及其水源水中3-硝基苯胺的定量检测,覆盖水样前处理、仪器分析及质控流程。
核心检测方法
液相色谱-串联质谱法(LC-MS/MS):通过色谱分离与质谱多重反应监测(MRM)模式,实现痕量3-硝基苯胺的高灵敏度测定。
检出限与定量限
检出限(LOD)为0.02 μg/L,定量限(LOQ)为0.05 μg/L,满足饮用水卫生标准中痕量污染物的管控要求。
质控样品要求
每批次检测需包含空白样、平行样及加标回收样:空白样中目标物不得检出;平行样相对偏差≤20%;加标回收率范围为70%-130%。
关键实验步骤
1. 水样经固相萃取柱(C18或HLB)富集净化;
2. 氮吹浓缩后复溶至流动相体系;
3. LC-MS/MS分析时采用阳离子模式,母离子m/z 139→122/93作为定性定量离子对。
特别说明
3-硝基苯胺易光解,实验全程需避光操作;标准储备液需用棕色瓶保存(-20℃),使用前需验证纯度及稳定性。

以上信息仅供参考,请以相应标准的原文为准!