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己酸乙酯_123-66-0,己酸乙酯
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己酸乙酯

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己酸乙酯介绍:

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Instrument

GC/FID

Method Details

Detection

FID

Initial Temp:250℃/8min,End Temp:250℃, Gradient: 10℃/min

Column

HP-5(25m*0.25mm*0.25µm)

Flow

1.5 mL/min

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.

Tel:029-85836892 Web:www.qjbzwz.com Email:qjbzwz@qjbzwz.com

Address:Jiawei Technology Industry Base, Aerospace East Road, Xi’an , Shaanxi Province


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

1. 标准名称及标准号
GB 5009.262-2016 食品安全国家标准 食品中甲酸、乙酸、丙酸、己酸、柠檬酸、乳酸、苹果酸的测定
2. 适用范围
适用于食品(如酒类、调味品等)中己酸及其酯类(包括己酸乙酯)的定量分析。
3. 核心检测方法
气相色谱法(GC):样品经预处理后,使用气相色谱仪分离目标物质,通过保留时间和质谱比对定性,外标法定量。
4. 检出限与定量限
己酸乙酯的检出限(LOD)为0.1 mg/kg,定量限(LOQ)为0.3 mg/kg。
5. 质控样品要求
1. 空白样品:需确保无目标物残留;
2. 加标回收率:80%-110%;
3. 平行样偏差:相对标准偏差(RSD)≤10%。
6. 关键实验步骤
1. 样品预处理:液液萃取或固相萃取富集目标物;
2. 色谱条件:选用极性毛细管色谱柱(如DB-WAX),进样口温度250℃,检测器温度280℃;
3. 定性与定量:通过标准品比对及质谱数据库匹配。
7. 特别说明
1. 避免使用塑料容器:己酸乙酯易吸附于塑料表面;
2. 需定期校准仪器,确保色谱峰分离度≥1.5;
3. 若样品基质复杂,可改用气相色谱-质谱联用(GC-MS)提高准确性。

以上信息仅供参考,请以相应标准的原文为准!