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乙酸乙酯_
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乙酸乙酯

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乙酸乙酯介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Ethyl acetate

Product Code

BW901039

Lot Number

23111514

CAS No.

141-78-6

Mol. Formula

C4H8O2

Mol. Weight

88.11

Certified on

14 Nov 2023

Expiry Date

13 Nov 2028

Storage Temp

4°C ± 4°C

Specification

100mg

CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.7%

1.0%

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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本公司销售的所有产品仅供实验科研使用,不用于人体及临床诊断。

标准名称及标准号
GB/T 12717-2022 工业用乙酸酯类试验方法
适用范围
本标准适用于工业用乙酸乙酯、乙酸丙酯等酯类产品的纯度、水分、酸度及其他杂质的检测,适用于产品质量控制和验收。
核心检测方法
气相色谱法(GC) 通过色谱柱分离乙酸乙酯中的组分,利用检测器(如FID)定量分析主成分及杂质。
检出限与定量限
杂质检测 检出限≤0.01%(质量分数),定量限≤0.03%(质量分数)。
质控样品要求
加标回收率 应控制在90%-110%,每批次样品须包含空白样和平行样。
关键实验步骤
1. 样品制备 准确称取样品,用适当溶剂稀释后进样。
2. 色谱条件 色谱柱为极性毛细管柱,载气为氮气,流速1.0 mL/min。
特别说明
检测环境 实验场所应通风良好,避免乙酸乙酯挥发造成浓度超标风险。

以上信息仅供参考,请以相应标准的原文为准!