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毒死蜱(EC 17025)_2921-88-2,毒死蜱
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毒死蜱(EC 17025)

BW902043 {{goodObj.price > 0 ? '¥' + goodObj.price : '咨询'}} ¥{{goodObj.sell_price || 0}} 咨询 2921-88-2 10mg {{goodObj.date}} 秦境标物 {{item.norm}} 99.8% {{inventory}}
毒死蜱介绍:

REFERENCE MATERIAL CERTIFICATE

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO9001.

Product Name

Chlorpyrifos

Product Code

BW902043

Lot Number

23091502

CAS No.

2921-88-2

Mol. Formula

C9H11Cl3NO3PS

Mol. Weight

350.59

Certified on

2 Sep 2023

Expiry Date

1 Sep 2026

Storage Temp

4°C ± 4°C

Specification

10mg


CERTIFIED

Purity

CERTIFIED

Expanded Uncertainty (U)

Approved by

99.8%

1.0%

Method of Characterisation

GC/FID

Batch Information

Water Content: <0.1% (by Karl-Fischer-Titration)

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of characterisation, homogeneity and stability testing. Stability values are based on real evidence opposed to simulation.

The producer certifies that this reference material meets the specification stated in this certificate until the expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for this reference material are set out in the terms and conditions of purchase.

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Safety

Proper precautions should be observed while handling. See Safety Data Sheet.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards (DKD). The calibration of the balances is verified daily internally and annually by an external accredited calibration service. Chromatographic methods are traceable to the International System of Units (SI).

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity compliant with ISO 17034.

Storage

The RM should be stored in the original sealed container at the indicated temperature.

Instructions for use

It is recommended to use 1 mg as the minimum sample size and if less material is used, to increase the certified uncertainty by a factor of two for half sample and four for a quarter of sample. If storage after opening is necessary, the RM should be tightly closed and kept from light and moisture. If the RM was in a sealed ampoule, it should be transferred to a vial with minimum head space.


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国家标准解读:
标准名称及标准号 食品安全国家标准 植物源性食品中毒死蜱残留量的测定 气相色谱-质谱法(GB 23200.113-2018
适用范围 适用于植物源性食品(如谷物、蔬菜、水果等)中毒死蜱残留量的测定。
核心检测方法 采用气相色谱-质谱联用(GC-MS)技术,通过内标法或外标法定量,结合基质匹配校准消除基质效应。
检出限与定量限 检出限(LOD)为0.01 mg/kg,定量限(LOQ)为0.05 mg/kg。
质控样品要求 每批次样品需包含空白样品、加标回收样(加标量为LOQ至10倍LOQ)和实际样品平行样,加标回收率需在70%-120%范围内。
关键实验步骤 1. 样品经乙腈提取后盐析分层;
2. 使用分散固相萃取(QuEChERS)净化;
3. 浓缩定容后进样;
4. GC-MS分析(色谱柱:DB-5MS,分流/不分流进样模式)。
特别说明 1. 避免使用含氯化钠的盐析包,以防对色谱柱造成损害;
2. 质谱监测需选择特征离子(如毒死蜱定量离子为197,定性离子为314、258)。

以上信息仅供参考,请以相应标准的原文为准!