GB 31658.17-2021 食品安全国家标准 动物性食品中四环素类、磺胺类和喹诺酮类药物残留量的测定 液相色谱－串联质谱法
颁发部门：农业农村部,国家卫生健康委员会,国家市场监督管理总局
标签：
环丙沙星
,
氧氟沙星
GB 31658.17-2021 | GB 31658.17-2021 食品安全国家标准 动物性食品中四环素类、磺胺类和喹诺酮类药物残留量的测定 液相色谱－串联质谱法 现行
发布日期：2021-09-16 实施日期：2022-02-01
GB 31658.17-2021相关产品
| 商城编码 | 产品名称 | 标准值 | 规格 | CAS号 | 有效期 | 库存 | 标准价 | 数量 | 操作 |
|---|---|---|---|---|---|---|---|---|---|
|
见证书
|
10g
|
0
|
1200.0
|
|
|||||
|
见证书
|
10g
|
0
|
1600.0
|
|
|||||
|
见证书
|
10g
|
0
|
800.0
|
|
|||||
|
见证书
|
10g
|
0
|
1200.0
|
|
|||||
|
见证书
|
10g
|
0
|
1200.0
|
|
|||||
|
（μg/kg） 88.9
|
10g
|
0
|
1000.0
|
|
|||||
|
（ug/kg） 恩诺沙星 89.8 环丙沙星 90.5
|
10g
|
0
|
1200.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
950.0
|
|
|||||
|
100μg/mL
|
1ml
|
0
|
1000.0
|
|
|||||
|
100µg/mL
|
3*1ml
|
0
|
2310.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
1034.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
855.0
|
|
|||||
|
1000μg/mL
|
1.2mL
|
115550-35-1
|
0
|
216.0
|
|
||||
|
98.6%
|
100mg
|
74011-58-8
|
2028-05-28
|
10
|
180.0
|
|
|||
|
1000μg/mL
|
1.2mL
|
98105-99-8
|
2027-05-07
|
10
|
120.0
|
|
|||
|
1000μg/mL
|
1.2mL
|
70458-92-3
|
2026-12-08
|
6
|
276.0
|
|
|||
|
100μg/mL
|
1.2mL
|
0
|
648.0
|
|
|||||
|
100μg/mL
|
1.2mL
|
0
|
720.0
|
|
|||||
|
1000μg/mL
|
1.2mL
|
98106-17-3
|
0
|
180.0
|
|
||||
|
100μg/mL
|
1.2mL
|
2026-11-08
|
9
|
960.0
|
|
||||
|
10μg/mL
|
1.2mL
|
2026-06-25
|
10
|
960.0
|
|
||||
|
13组分
|
1.2mL
|
0
|
600.0
|
|
|||||
|
1000μg/mL
|
1.2mL
|
82419-36-1
|
2026-05-21
|
10
|
120.0
|
|
|||
|
1000μg/mL
|
1.2mL
|
112398-08-0
|
2027-03-23
|
10
|
120.0
|
|
|||
|
100μg/mL
|
1.2mL
|
0
|
960.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
1122.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
1170.0
|
|
|||||
|
见产品详情
|
20g
|
2026-03-22
|
9
|
2600.0
|
|
||||
|
见证书
|
10g
|
0
|
900.0
|
|
|||||
|
见证书
|
10g
|
0
|
1200.0
|
|
|||||
|
见证书
|
10g
|
0
|
2200.0
|
|
|||||
|
GB31658.17-2021
|
20g
|
0
|
16800.0
|
|
|||||
|
GB31658.17-2021
|
20g
|
0
|
15120.0
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
248.0
|
|
|||||
|
100μg
|
100µg*4/vial
|
0
|
660.0
|
|
|||||
|
150mg/6mL
|
30支/盒
|
0
|
600.0
|
|
|||||
|
200mg/6mL
|
30支/盒
|
0
|
600.0
|
|
|||||
|
1000mg/6mL
|
30支/盒
|
0
|
1800.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
见产品详情
|
10g
|
0
|
4800.0
|
|
|||||
|
见产品详情
|
10g
|
0
|
2000.0
|
|
|||||
|
见产品详情
|
10g
|
0
|
2200.0
|
|
|||||
|
4组分
|
15g
|
0
|
1680.0
|
|
|||||
|
15组分
|
10g
|
0
|
4920.0
|
|
|||||
|
17组分
|
10g
|
0
|
5520.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
3组分
|
10g
|
0
|
1320.0
|
|
|||||
|
125μg/kg
|
10g
|
93106-60-6
|
0
|
720.0
|
|
||||
|
44.7μg/kg
|
10g
|
98106-17-3
|
0
|
720.0
|
|
||||
|
13组分
|
10g
|
0
|
4320.0
|
|
|||||
|
4组分
|
10g
|
0
|
1680.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
4组分
|
10g
|
0
|
1320.0
|
|
|||||
|
4组分
|
10g
|
0
|
1320.0
|
|
|||||
|
4组分
|
10g
|
0
|
1680.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
22组分
|
10g
|
0
|
7080.0
|
|
|||||
|
11组分
|
10g
|
0
|
3720.0
|
|
|||||
|
13组分
|
10g
|
0
|
4200.0
|
|
|||||
|
11组分
|
10g
|
0
|
4080.0
|
|
|||||
|
12组分
|
10g
|
0
|
4080.0
|
|
|||||
|
21组分
|
10g
|
0
|
6720.0
|
|
|||||
|
4组分
|
10g
|
0
|
1080.0
|
|
|||||
|
4组分
|
10g
|
2027-07-01
|
2
|
1080.0
|
|
||||
|
4组分
|
10g
|
0
|
1680.0
|
|
|||||
|
242μg/kg
|
10g
|
0
|
720.0
|
|
|||||
|
100μg/mL
|
1.2mL
|
122-16-7
|
2026-06-18
|
10
|
60.0
|
|
|||
|
10μg/mL
|
1mL
|
0
|
440.0
|
|
|||||
|
见产品详情
|
10g
|
2026-06-26
|
20
|
2200.0
|
|
||||
|
见证书
|
6g
|
0
|
咨询
|
|
|||||
|
见证书
|
6g
|
0
|
咨询
|
|
|||||
|
见证书
|
6g
|
0
|
咨询
|
|
|||||
|
1.002mol/L
|
500mL
|
1310-73-2
|
0
|
108.0
|
|
||||
|
1mol/L
|
100mL
|
1310-73-2
|
0
|
60.0
|
|
||||
|
见证书
|
10g
|
0
|
2000.0
|
|
|||||
|
见证书
|
200g
|
0
|
咨询
|
|
|||||
|
303μg/Kg
|
10g
|
93106-60-6
|
0
|
750.0
|
|
||||
|
磺胺间甲氧嘧啶：57.3μg/kg;磺胺甲噁唑：52.9μg/kg;磺胺二甲嘧啶：48.4μg/kg;氟苯尼考：87.8μg/kg;氟苯尼考胺：49.3μg/kg
|
15g
|
0
|
2500.0
|
|
|||||
|
未检出*
|
10g
|
93106-60-6
|
0
|
750.0
|
|
||||
|
100μg/ml
|
1.2ml
|
0
|
900.0
|
|
|||||
|
见产品详情
|
10g
|
2026-06-15
|
2
|
2600.0
|
|
||||
|
见证书
|
50g
|
0
|
12300.0
|
|
|||||
|
87.4µg/kg
|
20g
|
2026-06-15
|
1
|
800.0
|
|
||||
|
99.4%
|
10mg
|
852-19-7
|
2026-07-17
|
7
|
626.0
|
|
|||
|
57.5μg/kg
|
10g
|
2026-06-03
|
2
|
800.0
|
|
||||
|
见产品详情
|
10g
|
0
|
2200.0
|
|
|||||
|
未检出
|
20g
|
2027-07-19
|
91
|
1600.0
|
|
||||
|
见产品详情
|
20g
|
2026-07-19
|
79
|
3000.0
|
|
||||
|
未检出
|
20g
|
2027-07-19
|
1
|
3600.0
|
|
||||
|
见产品详情
|
10g
|
2026-05-28
|
1
|
1400.0
|
|
||||
|
见产品详情
|
10g
|
2026-07-19
|
1
|
2000.0
|
|
||||
|
见产品详情
|
10g
|
0
|
1600.0
|
|
|||||
|
未检出
|
10g
|
2027-08-08
|
15
|
800.0
|
|
||||
|
未检出
|
10g
|
2027-08-08
|
20
|
2600.0
|
|
||||
|
未检出
|
10g
|
2027-08-08
|
20
|
2200.0
|
|
||||
|
239µg/kg
|
10g
|
2026-05-28
|
1
|
800.0
|
|
||||
|
141.0μg/kg
|
10g
|
0
|
801.0
|
|
|||||
|
221.0μg/kg
|
10g
|
93106-60-6
|
0
|
800.0
|
|
||||
|
659.0μg/kg
|
10g
|
93106-60-6
|
0
|
800.0
|
|
||||
|
见产品详情
|
10g
|
2026-09-01
|
12
|
3400.0
|
|
||||
|
100μg/mL
|
1mL
|
2028-05-22
|
131
|
咨询
|
|
||||
|
100μg/mL
|
1mL
|
2028-01-15
|
126
|
咨询
|
|
||||
|
见证书
|
100μg/组分
|
2028-06-08
|
159
|
咨询
|
|
||||
|
见产品详情
|
10g
|
2026-09-09
|
14
|
1200.0
|
|
||||
|
12组分
|
10g
|
0
|
4920.0
|
|
|||||
|
见产品详情
|
10g
|
2026-09-03
|
13
|
1800.0
|
|
||||
|
见证书
|
10g
|
0
|
咨询
|
|
|||||
|
见证书
|
10g
|
0
|
咨询
|
|
|||||
|
见证书
|
10g
|
0
|
咨询
|
|
|||||
|
见证书
|
15g
|
0
|
咨询
|
|
|||||
|
见证书
|
20g
|
68-35-9
|
0
|
咨询
|
|
||||
|
见证书
|
20g
|
0
|
咨询
|
|
|||||
|
见证书
|
10g
|
0
|
1200.0
|
|
|||||
|
≥95%
|
250mg
|
2058-46-0
|
0
|
683.0
|
|
||||
|
98%
|
1g
|
7477-67-0
|
0
|
68.0
|
|
||||
|
98%
|
100g
|
41825-73-4
|
0
|
1027.0
|
|
||||
|
97%
|
1g
|
38762-41-3
|
0
|
23.0
|
|
||||
|
122±25μg/kg
|
10g/瓶
|
2022-01-01
|
10
|
850.0
|
|
||||
|
磺胺嘧啶101±21磺胺索嘧啶103±21磺胺吡啶104±21磺胺二甲嘧啶104±21（μg/kg）
|
10g/瓶
|
2025-01-01
|
10
|
1750.0
|
|
||||
|
磺胺嘧啶40.2±8.1 μg/kg
|
10g/瓶
|
2027-01-01
|
10
|
850.0
|
|
||||
|
磺胺邻二甲氧嘧啶 100± 20磺胺甲恶唑 102± 21磺胺甲基嘧啶 103 ±21磺胺二甲嘧啶 104 ±21磺胺间甲氧嘧啶 107± 22甲氧苄啶 100 ±20磺胺间二甲氧嘧啶 107 ±22磺胺喹恶啉 96±
|
10g/瓶
|
2026-01-01
|
10
|
4150.0
|
|
||||
|
磺胺间甲氧嘧啶34.1±6.9（μg/kg）
|
10g/瓶
|
2025-01-01
|
10
|
850.0
|
|
||||
|
磺胺甲恶唑39.4±9.9 磺胺二甲嘧啶41.6±10.4 磺胺间甲氧嘧啶37.3±9.4 磺胺喹恶啉34.8±8.7 磺胺嘧啶40.2±10.1（μg/kg）
|
10g/瓶
|
2026-01-01
|
10
|
2050.0
|
|
||||
|
磺胺间二甲氧嘧啶 104.7±20.9 磺胺邻二甲氧嘧啶107±21.4（ug/kg）
|
10g/瓶
|
2022-01-01
|
10
|
1300.0
|
|
||||
|
磺胺嘧啶107±22 磺胺索嘧啶77.8±15.8 磺胺吡啶38.4±7.7 磺胺二甲嘧啶127±26μg/kg
|
10g/瓶
|
2026-01-01
|
10
|
1800.0
|
|
||||
|
磺胺二甲基嘧啶:127±26 μg/kg 磺胺间甲氧嘧啶 107±22 μg/kg
|
10g/瓶
|
2027-01-01
|
10
|
1250.0
|
|
||||
|
磺胺邻二甲氧嘧啶103±21磺胺甲恶唑109±22磺胺甲基嘧啶102±21磺胺二甲嘧啶127±26磺胺间甲氧嘧啶107±22甲氧苄啶95±19磺胺间二甲氧嘧啶111±23磺胺喹恶啉113±23磺胺嘧啶107±22磺胺氯哒嗪121±25磺胺氯吡嗪126±26磺胺甲氧哒嗪118±24（μg/kg）
|
10g/瓶
|
2027-01-01
|
10
|
4150.0
|
|
||||
|
磺胺二甲基嘧啶65±13（μg/kg）
|
10g/瓶
|
2025-01-01
|
10
|
850.0
|
|
||||
|
磺胺甲恶唑109±22 磺胺二甲嘧啶127±26 磺胺间甲氧嘧啶107±22 磺胺喹恶啉113±23 磺胺间二甲氧嘧啶111±23（μg/kg）
|
10g/瓶
|
2026-01-01
|
10
|
2050.0
|
|
||||
|
磺胺间甲氧嘧啶39.6±8.0 磺胺二甲嘧啶40.4±8.1 磺胺嘧啶46.4±9.3 磺胺甲恶唑 44.0±8.8（μg/kg）
|
30g
|
2025-01-01
|
10
|
2300.0
|
|
||||
|
磺胺甲基嘧啶 35.3±7.1磺胺二甲基嘧啶34.8±7.0磺胺间甲氧嘧啶34.1±6.9磺胺喹恶啉34.8±7.0磺胺嘧啶 40.2±8.1（μg/kg）
|
10g/瓶
|
2025-01-01
|
10
|
2050.0
|
|
||||
|
磺胺间甲氧嘧啶 126 ±26磺胺二甲嘧啶 157± 78± 16磺胺间二甲氧嘧啶 103 ±21磺胺喹恶啉 85 ±17 μg/kg
|
10g/瓶
|
2027-01-01
|
10
|
2100.0
|
|
||||
|
磺胺嘧啶48.6±9.8、磺胺二甲嘧啶47.1±9.5 ug/kg
|
10g/瓶
|
2026-01-01
|
10
|
1250.0
|
|
||||
|
磺胺邻二甲氧嘧啶101±21 磺胺甲恶唑97±20 磺胺甲基嘧啶100±20 磺胺二甲嘧啶106±22 磺胺间甲氧嘧啶94±19 甲氧苄啶104±21 磺胺间二甲氧嘧啶101±21 磺胺喹恶啉88±18 磺胺嘧啶105±21 磺胺氯哒嗪102±21 磺胺氯吡嗪95±19 磺胺甲氧哒嗪87±18（μg/kg）
|
10g/瓶
|
2026-01-01
|
10
|
4150.0
|
|
||||
|
磺胺噻唑9.4±1.9磺胺异恶唑 10.3±2.1磺胺二甲嘧啶9.6±1.9磺胺嘧啶9.7±1.9磺胺甲恶唑10.4±2.1磺胺喹噁啉10.1±2.0磺胺间二甲氧嘧啶 9.4±1.9磺胺甲基嘧啶10.3±2.1（μg/kg）
|
10g/瓶
|
2025-01-01
|
10
|
2950.0
|
|
||||
|
见证书
|
10g/瓶
|
2025-01-01
|
10
|
850.0
|
|
||||
|
磺胺二甲基嘧啶 191±39 磺胺嘧啶 198±40 （ug/kg）
|
10g/瓶
|
2025-01-01
|
10
|
1250.0
|
|
||||
|
磺胺二甲嘧啶104±21（μg/kg）
|
10g/瓶
|
2027-01-01
|
10
|
850.0
|
|
||||
|
未检出
|
10g/瓶
|
2025-01-01
|
10
|
2250.0
|
|
||||
|
磺胺甲基异噁唑（磺胺甲噁唑） 65.0±13.0（μg/kg）
|
10g/瓶
|
2026-01-01
|
10
|
850.0
|
|
||||
|
磺胺嘧啶 44±9 多西环素 50±10（μg/kg）
|
20g/袋
|
2026-01-01
|
10
|
1875.0
|
|
||||
|
99%
|
25mg
|
345627-80-7
|
0
|
584.0
|
|
||||
|
95%
|
1g
|
3457-48-5
|
0
|
48.0
|
|
||||
|
average Mw ~800,average Mn ~600
|
10ml
|
25987-06-8
|
0
|
63.0
|
|
||||
|
98%
|
500g
|
25990-60-7
|
0
|
2156.0
|
|
||||
|
99%
|
25g
|
132123-39-8
|
0
|
456.0
|
|
||||
|
98%
|
100g
|
5301-78-0
|
0
|
566.0
|
|
||||
|
见证书
|
10g瓶
|
0
|
1250.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
1250.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
2100.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
2650.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
1250.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
1250.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
2650.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
640.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
1650.0
|
|
|||||
|
见证书
|
10g/瓶
|
0
|
560.0
|
|
|||||
|
见证书
|
10g/袋
|
0
|
850.0
|
|
|||||
|
见证书
|
10g/袋
|
0
|
850.0
|
|
|||||
|
见证书
|
20g/袋
|
0
|
640.0
|
|
|||||
|
99.7%
|
250mg
|
127-69-5
|
2030-10-31
|
10
|
174.0
|
|
|||
|
见产品详情
|
10g
|
0
|
2200.0
|
|
|||||
|
见产品详情
|
10g
|
2026-07-24
|
55
|
1600.0
|
|
||||
|
HLB 150mg/6mL
|
30支/盒
|
0
|
626.0
|
|
|||||
|
HLB 200mg/6mL
|
30支/盒
|
0
|
740.0
|
|
|||||
|
10ug/mL
|
1mL
|
0
|
1500.0
|
|
|||||
|
10μg/mL
|
1mL
|
0
|
咨询
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
咨询
|
|
|||||
|
100μg/mL
|
1mL
|
0
|
咨询
|
|
|||||
|
见证书
|
1套
|
0
|
咨询
|
|
|||||
|
33.0µg/kg
|
10g
|
2026-12-11
|
10
|
800.0
|
|
||||
|
56.0µg/kg
|
10g
|
2026-12-11
|
9
|
1000.0
|
|
||||
|
50.4µg/kg
|
10g
|
2026-12-11
|
14
|
1000.0
|
|
||||
|
0.0332mg/kg
|
10g
|
2026-07-24
|
2
|
800.0
|
|
||||
|
见证书
|
20g
|
0
|
5100.0
|
|
|||||
|
见产品详情
|
10g
|
2026-11-27
|
4
|
1600.0
|
|
||||
|
见产品详情
|
10g
|
2026-11-27
|
52
|
1600.0
|
|
||||
|
pH=5.0
|
500mL
|
0
|
336.0
|
|
|||||
|
pH=5.0
|
1000mL
|
0
|
532.0
|
|